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71.
Junjun Chen Jian Chen Xiumin Yao Zhongming Chen Xuejian Liu Zhengren Huang 《Journal of the European Ceramic Society》2018,38(9):3083-3088
SiC/20?wt% ZrB2 composite ceramics were fabricated via pressureless solid phase sintering in argon atmosphere at different temperature. The effect of sintering temperature on microstructure, electrical properties and mechanical properties of SiC/ZrB2 ceramics was investigated. Electrical resistivity exhibits twice significant decreases with increasing sintering temperature. The first decrease from 1900?°C to 2000?°C is attributed to the obvious decrease of continuous pore channels in as-sintered materials. The second decrease from 2100?°C to 2200?°C results from the improvement of carbon crystallization and the disappearance of amorphous layers enveloping ZrB2 grains. Additionally, the increase of sintered density with increasing temperature caused greatly advance of flexural strength, elastic modulus and Vickers hardness. But excessive temperature is detrimental to flexural strength because of SiC grain growth. 相似文献
72.
Li-Feng Zhu Bo-Ping Zhang Jia-Qi Duan Bo-Wei Xun Ning Wang Yu-Cheng Tang Gao-Lei Zhao 《Journal of the European Ceramic Society》2018,38(10):3463-3471
0.7BiFeO3-0.3BaTiO3 (BFO-0.3BT) ceramics were prepared to uncover the impacts of sintering temperature (TS) and dwell time (td) on the microstructure and electrical properties. With increasing the TS or td, the grain sizes increase along with the porosity decreases, which is in favor of the alignment of dipole. However, excess TS or td are inclined to cause the volatilization of Bi2O3, which deteriorates piezoelectric properties. Because of the R-T two-phase coexistence, low defect ions concentration and porosity, as well as appropriate grain size, the excellent d33?=?208?pC/N and kp?=?35.46% as well as Pr?=?28.52?μC/cm2 were achieved in BFO-0.3BT ceramics at TS?=?1000?°C and td?=?6?h. In addition,large unipolar strain 0.13% and d33*?=?256.2?pm/V also were obtained in BFO-0.3BT ceramics at TS?=?1000?°C and td?=?6?h. This research indicates that the porosity and defect ion concentration as well as grain size also play an important role in piezoelectric properties in BFO-BT ceramics. 相似文献
73.
Zhuang Tang Yuwei Huang Kangning Wu Jianying Li 《Journal of the European Ceramic Society》2018,38(4):1569-1575
Significantly enhanced breakdown field of 24.52 kV cm?1 as well as noteworthy nonlinear coefficient of 8.11 and low dielectric loss of 0.077 were obtained in Ca0.6Sr0.4Cu3Ti4O12 ceramic. It was proved from impedance spectra that improved breakdown field was attributed to enhanced grain boundary resistance and elevated Schottky barrier height, which was further found resulting from reduced donor densities in C-V measurements. In addition, it was found that the activation energy originated from oxygen vacancies was increased, indicating the generation of oxygen vacancies was suppressed. Since oxygen vacancies acted as donors in depletion layers, it is reasonable to deduce that the reduced donor density was mainly ascribed to the decreased oxygen vacancies. In conclusion, maximum integrated action of strong solid solution effect and weak Sr-stretching effect was achieved when Sr/Ca ratio is 40/60, leading to greatly elevated potential barrier height and enhanced breakdown field consequently. 相似文献
74.
Morphology,mechanical properties and electromagnetic shielding effectiveness of poly(styrene‐b‐ethylene‐ran‐butylene‐b‐styrene)/carbon nanotube nanocomposites: effects of maleic anhydride,carbon nanotube loading and processing method 下载免费PDF全文
Nanocomposites based on poly(styrene‐b‐ethylene‐ran‐butylene‐b‐styrene) (SEBS) and carbon nanotubes (CNTs) (SEBS/CNT) as well as SEBS grafted with maleic anhydride (SEBS‐MA)/CNT were successfully prepared for electromagnetic shielding applications. Both SEBS/CNT and SEBS‐MA/CNT nanocomposites were prepared by melt compounding and were post‐processed using two different techniques: tape extrusion and compression moulding. The different nanocomposites were characterized by Raman spectroscopy and rheological analysis. Their mechanical properties, electrical properties (10-2–105 Hz) and electromagnetic shielding effectiveness (8.2–12.4 GHz) were also evaluated. The results showed that the CNT loading amount, the presence of MA in the matrix and the shaping technique used strongly influence the final morphologies and properties of the nanocomposites. Whilst the nanocomposite containing 8 wt% CNTs prepared by compression moulding presented the highest electromagnetic shielding effectiveness (with a value of 56.73 dB, which corresponds to an attenuation of 99.9996% of the incident radiation), the nanocomposite containing 5 wt% CNTs prepared by tape extrusion presented the best balance between electromagnetic and mechanical properties and was a good candidate to be used as an efficient flexible electromagnetic interference shielding material. © 2018 Society of Chemical Industry 相似文献
75.
76.
Herein, electrically conductive natural and synthetic yarns through electrophoretic deposition (EPD) technique were fabricated. A parametric study on the conductivity enhancement of the yarns is carried out by Taguchi method. Using this method, the desirable conditions are determined by studying the effects of important parameters on the electrical conductivity of the yarns in the EPD coating process. Based on the L18 design of experiments table, the preferred combination of factors to obtain the highest electrical conductivity of the yarns is found by Taguchi analysis. In addition, the Pareto ANOVA analysis is conducted to identify the major contributing factors on the electrical conductivity of the yarns. Characterisation techniques, such as scanning electron microscopy (SEM), Fourier transformed infrared spectroscopy (FTIR) in attenuated total reflectance (ATR) mode, and thermogravimetric analysis (TGA) are utilised for better understanding the microstructure and physical properties. When powered by only 3 V, the maximum temperature of a Joule heated conductive sample based on natural fibre yarns reached 102°C in less than 25 s. 相似文献
77.
《Ceramics International》2020,46(10):15991-15997
The ceramic (1-x)BiFe0.985Sc0.015O3-xBaZr0.2Ti0.8O3 + 1mol% MnO2 (x = 0.20, 0.25, 0.30, 0.35) (BFS-xBZT) was synthesized using the traditional ceramic sintering method. The components of the ceramic were determined by constructing a morphotropic phase boundary (MPB) which consists of rhombohedral (R) and tetragonal (T) phases (0.24≤ x ≤ 0.26). With the accumulation of BZT content, relax behaviors were observed by dielectric properties measurements. At the MPB, the crystal structures of the R phase and T phase change abruptly. The distortion degree of the R phase increases, and the differences between a and c of the T phase decrease. An enhanced ferroelectricity Pr of ~27.8 μC/cm2 and apex piezoelectric coefficient d33 of 131 ± 4 pC/N are obtained near the MPB (x = 0.25), due to the R-T phase coexistence near room temperature. The results show that BFS-xBZT ceramics could be a candidate for lead-free piezoelectric ceramics at high operating temperatures. 相似文献
78.
申建光 《工业仪表与自动化装置》2020,(1):54-57,64
为提高环形供热管网水力工况运行稳定性,提出了基于模糊PID控制的环形供热管网水力工况控制方法。构建环形供热管网水力工况控制的约束参量模型,在此基础上采用回归模型逼近方法构建其测试指标集,结合自适应融合反馈跟踪方法进行环形供热管网水力工况信息的融合处理,并从中提取分布特征量;采用模糊PID控制方法调节提取结果的输出稳定性,实现环形供热管网水力工况优化设计和自适应控制。仿真结果表明,采用该方法进行环形供热管网水力工况控制的稳定性较好,自适应控制能力较强,实现了环形供热管网水力工况优化调节。 相似文献
79.
80.
Based on multiphase field conception and integrated with the idea of vectorvalued phase field, a phase field model for typical allotropic transformation of solid
solution is proposed. The model takes the non-uniform distribution of grain boundaries of
parent phase and crystal orientation into account in proper way, as being illustrated by the
simulation of austenite to ferrite transformation in low carbon steel. It is found that the
misorientation dependent grain boundary mobility shows strong influence on the
formation of ferrite morphology comparing with the weak effect exerted by
misorientation dependent grain boundary energy. The evolution of various types of grain
boundaries are quantitatively characterized in terms of its respective grain boundary
energy dissipation. The simulated ferrite fraction agrees well with the expectation from
phase diagram, which verifies this model. 相似文献